Microwave-Assisted One-Pot Synthesis of Octahydroquinazolinone Derivatives Catalyzed by Thiamine Hydrochloride Under Solvent-free Condition 


Vol. 55,  No. 6, pp. 936-939, Dec.  2011
10.5012/jkcs.2011.55.6.936


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  Abstract

Thiamine hydrochloride (VB1) has been used as an acid catalyst in organic synthesis. One pot three component Biginelli condensation of dimedone, urea/thiourea and substituted aromatic aldehydes catalyzed by 10 mol % of thiamine hydrochloride (VB1) in solvent free condition under microwave irradiation in good to excellent yields has been investigated. Utilization of microwave irradiation, simple reaction conditions, short reaction time, ease of product isolation, and purification makes this manipulation very interesting from an economic and environmental perspective.

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  Cite this article

[IEEE Style]

P. V. Badadhe, A. V. Chate, D. G. Hingane, P. S. Mahajan, N. M. Chavhan, C. H. Gill, "Microwave-Assisted One-Pot Synthesis of Octahydroquinazolinone Derivatives Catalyzed by Thiamine Hydrochloride Under Solvent-free Condition," Journal of the Korean Chemical Society, vol. 55, no. 6, pp. 936-939, 2011. DOI: 10.5012/jkcs.2011.55.6.936.

[ACM Style]

Pravin V Badadhe, Asha V Chate, Dattatraya G Hingane, Pravin S Mahajan, Namdev M Chavhan, and Charansingh H Gill. 2011. Microwave-Assisted One-Pot Synthesis of Octahydroquinazolinone Derivatives Catalyzed by Thiamine Hydrochloride Under Solvent-free Condition. Journal of the Korean Chemical Society, 55, 6, (2011), 936-939. DOI: 10.5012/jkcs.2011.55.6.936.

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ISSN(Print) 1017-2548
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